By Joseph Wang(auth.)

ISBN-10: 0471228230

ISBN-13: 9780471228233

ISBN-10: 0471282723

ISBN-13: 9780471282723

Content material:
Chapter 1 primary innovations (pages 1–27):
Chapter 2 research of Electrode Reactions (pages 28–59):
Chapter three Controlled?Potential concepts (pages 60–99):
Chapter four functional concerns (pages 100–139):
Chapter five Potentiometry (pages 140–170):
Chapter 6 Electrochemical Sensors (pages 171–202):

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Additional info for Analytical Electochemistry, Second Edition

Example text

G. Compton, Anal. , 72, 198A (2000). 5. D. Grahame, Chem. Rev. 41, 441 (1947). 6. A. Swietlow, M. Skoog, and G. Johansson, Electroanalysis, 4, 921 (1992). 7. C. Grahame, Annu. Rev. Phys. , 6, 337 (1955). 8. D. Mohilner, Electroanal. , 1, 241 (1966). 9. O'M. A. Devanathan, and K. Muller, Proc. R. , 55, A274 (1963). 10. R. Parsons, J. Electrochem. , 127, 176C (1980). 11. B. Mark, Analyst 115, 667 (1990). 12. M. Bond, I. Heritage, and M. Briggs, Langmuir, 1, 110 (1985). Questions 1. Show or draw the concentration pro®le/gradient near the electrode surface during a linear scan voltammetric experiment in stirred a solution.

A wide variety of fast reactions (including isomerization and dimerization) can thus be probed. The extraction of such information commonly requires background subtraction to correct for the large charging current contribution associated with ultrafast scan rates. A special case of the EC mechanism is the catalytic regeneration of O during the chemical step: O ‡ neÀ „ R …2-8† R‡A „ O …2-9† An example of such a catalytic EC process is the oxidation of dopamine in the presence of ascorbic acid (4).

1 Experimental Arrangement Optically transparent electrodes (OTEs), which enable light to be passed through their surface and the adjacent solution, are the keys for performing transmission 2-2 SPECTROELECTROCHEMISTRY 41 FIGURE 2-10 Thin-layer spectroelectrochemical cell. OTE ˆ optically transparent electrode. spectroelectrochemical experiments. One type of OTE consists of a metal (gold, silver, nickel) micromesh containing small (10±30 mm) holes, which couples good optical transmission (over 50%) with good electrical conductivity.

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Analytical Electochemistry, Second Edition by Joseph Wang(auth.)


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